4-Chloro-N-(3,5-dimethyl­phen­yl)benzene­sulfonamide

نویسندگان

  • K. Shakuntala
  • Sabine Foro
  • B. Thimme Gowda
چکیده

The asymmetric unit of the title compound, C(14)H(14)ClNO(2)S, contains two independent mol-ecules, which are twisted at the S atoms with C-SO(2)-NH-C torsion angles of -69.4 (7)° and 66.0 (8)°. The sulfonyl and the anilino benzene rings are tilted relative to each other by 49.0 (4) and 61.7 (3)° in the two mol-ecules. In the crystal, the mol-ecules are linked into chains by N-H⋯O hydrogen bonds.

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منابع مشابه

4-Chloro-N-(2,3-dimethyl­phen­yl)benzene­sulfonamide

In the title compound, C(14)H(14)ClNO(2)S, the two aromatic rings are tilted relative to each other by 34.7 (1)°. In the crystal, the mol-ecules form zigzag chains along the c axis via inter-molecular N-H⋯O hydrogen bonds.

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Crystal structures of isomeric 3,5-di­chloro-N-(2,3-di­methyl­phen­yl)benzene­sulfonamide, 3,5-di­chloro-N-(2,6-di­methyl­phen­yl)benzene­sulfonamide and 3,5-di­chloro-N-(3,5-di­methyl­phen­yl)benzene­sulfonamide

The crystal structures of three isomeric compounds of formula C14H13Cl2NO2S, namely 3,5-di-chloro-N-(2,3-di-methyl-phen-yl)-benzene-sulfonamide (I), 3,5-di-chloro-N-(2,6-di-methyl-phen-yl)benzene-sulfonamide (II) and 3,5-di-chloro-N-(3,5-di-methyl-phen-yl)benzene-sulfonamide (III) are described. The mol-ecules of all the three compounds are U-shaped with the two aromatic rings inclined at 41.3 ...

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4-Chloro-N-(3,4-dimethyl­phen­yl)benzene­sulfonamide

In the title compound, C(14)H(14)ClNO(2)S, the angle between the sulfonyl and aniline benzene rings is 65.5 (1)°. The crystal structure features inversion dimers linked by pairs of N-H⋯O hydrogen bonds. The dimethyl-phenyl ring is disordered over two different orientations approximately related by a 180° rotation about the C-N bond, with occupancies of 0.643 (6) and 0.357 (6).

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4-Chloro-N-(2,5-dimethyl­phen­yl)benzene­sulfonamide

The title compound, C(14)H(14)ClNO(2)S, contains two molecules in the asymmetric unit with different conformations. The C-SO(2)-NH-C torsion angles are 65.3 (2) and 54.6 (2)° and the aromatic rings are tilted relative to each other by 59.3 (1) and 45.8 (1)° in the two mol-ecules. In the crystal, inversion symmetry results in dimers linked by pairs of N-H⋯O hydrogen bonds for both molecules.

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N-(3,5-Dimethyl­phen­yl)benzene­sulfonamide

In the crystal structure of the title compound, C(14)H(15)NO(2)S, the mol-ecule is bent at the S atom with a C-SO(2)-NH-C torsion angle of 67.9 (2)°. The two benzene rings are tilted by 54.6 (1)° relative to each other. In the crystal, inter-molecular N-H⋯O hydrogen bonds pack the mol-ecules into a supra-molecular structure.

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عنوان ژورنال:

دوره 67  شماره 

صفحات  -

تاریخ انتشار 2011